Detection of secondary amines on solid phase.

  title={Detection of secondary amines on solid phase.},
  author={T Vojkovsky},
  journal={Peptide research},
  volume={8 4},
The detection of secondary amino groups in building blocks attached to solid phase using tetrachlorobenzoquinone (chloranil) was re-examined. A new procedure, about ten times more sensitive than the original method, has been developed. Except for N(p-tolyl)glycine, all secondary amino groups that were examined were detected reliably in a substitution range down to 2.8 micro eq/g. Protected imidazole in His(Trt) did not interfere with the detection method. 
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Journal of peptide science : an official publication of the European Peptide Society • 2001
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