Detailed analysis of the S-RESPDOR solid-state NMR method for inter-nuclear distance measurement between spin-1/2 and quadrupolar nuclei.

@article{Lu2012DetailedAO,
  title={Detailed analysis of the S-RESPDOR solid-state NMR method for inter-nuclear distance measurement between spin-1/2 and quadrupolar nuclei.},
  author={Xingyu Lu and Olivier Lafon and Julien Tr{\'e}bosc and Jean Paul Amoureux},
  journal={Journal of magnetic resonance},
  year={2012},
  volume={215},
  pages={34-49}
}
We present a detailed analysis of the Symmetry-based Resonance-Echo Saturation-Pulse DOuble-Resonance (S-RESPDOR) method in order to measure the inter-nuclear distances between spin-1/2 and quadrupolar nuclei. This recently introduced sequence employs a symmetry-based recoupling scheme on the observed spin-1/2 channel and a saturation pulse on the quadrupolar channel. This method requires a low radio-frequency (rf) field, is compatible with high MAS frequency and allows a rapid determination of… CONTINUE READING
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