Crystal structure of hexaaquamagnesium(II) diperchlorate diadamantane dihydrate, [Mg(H2O)6][ClO4]2 · 2C10H16 · 2H2O

@article{Tai2007CrystalSO,
  title={Crystal structure of hexaaquamagnesium(II) diperchlorate diadamantane dihydrate, [Mg(H2O)6][ClO4]2 · 2C10H16 · 2H2O},
  author={Xi-Shi Tai and Jie Yin and Ming-Yang Hao},
  journal={Zeitschrift f{\"u}r Kristallographie - New Crystal Structures},
  year={2007},
  volume={222},
  pages={231 - 232}
}
C20H48Cl2MgO16, triclinic, P1 (no. 2), a = 8.251(4) Å, b = 9.230(4) Å, c = 10.784(5) Å, 0 = 94.047(8)°, 1 = 104.358(8)°, " = 114.193(8)°, V = 711.9 Å, Z = 1, Rgt(F) = 0.074, wRref(F) = 0.223, T = 294 K. Source of material All commercially available reagentswere used as supplied.A solution of adamantane (10mmol) in 95% ethanol (10ml) was added slowly to a solution ofmagnesium perchlorate (10mmol) in 95% ethanol. The reaction mixture was stirred for 4 h, then the resulting solutionwas slowly… CONTINUE READING

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