Comparison of extraction and clean-up procedures for analysis of zearalenone in corn, rice and wheat grains by high-performance liquid chromatography with photodiode array and fluorescence detection.

@article{Llorens2002ComparisonOE,
  title={Comparison of extraction and clean-up procedures for analysis of zearalenone in corn, rice and wheat grains by high-performance liquid chromatography with photodiode array and fluorescence detection.},
  author={Amparo Llorens and Rufino Mateo and Jos{\'e} Juan Mateo and Misericordia Jim{\'e}nez},
  journal={Food additives and contaminants},
  year={2002},
  volume={19 3},
  pages={272-81}
}
The aim of this work was the optimization of some procedures usually used in the analysis of zearalenone (ZEA) in corn and other cereals by high-performance liquid chromatography (HPLC) with photodiode array and/or fluorescence detection. The comparison of five extraction solvents is presented. Three solid-phase extraction cartridges (C-18, silica, Florisil) and immuno-affinity columns were also compared to obtain the best recovery of the mycotoxin with the minimal presence of co-extractives in… CONTINUE READING
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