Chemical tagging of chlorinated phenols for their facile detection and analysis by NMR spectroscopy.


A derivatization method that employs diethyl (bromodifluoromethyl) phosphonate (DBDFP) to efficiently tag the endocrine disruptor pentachlorophenol (PCP) and other chlorinated phenols (CPs) along with their reliable detection and analysis by NMR is presented. The method accomplishes the efficient alkylation of the hydroxyl group in CPs with the… (More)
DOI: 10.1007/s00216-015-8625-2


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