Characterization and structure determination of ammonium bismuth oxalate hydrate, Bi(NH(4))(C(2)O(4))(2).xH(2)O.

@article{Vanhoyland2004CharacterizationAS,
  title={Characterization and structure determination of ammonium bismuth oxalate hydrate, Bi(NH(4))(C(2)O(4))(2).xH(2)O.},
  author={G. Vanhoyland and Armel Le Bail and Jules Mullens and Lucien C Van Poucke},
  journal={Inorganic chemistry},
  year={2004},
  volume={43 2},
  pages={785-9}
}
From on-line coupled TGA-MS and TGA-FTIR measurements, in combination with a quantitative chemical analysis, it was deduced that the chemical formula for an unknown bismuth oxalate compound had to be Bi(NH(4))(C(2)O(4))(2).3.71(6)H(2)O. Solution of the crystallographic structure on the basis of X-ray powder data proved this formula to be correct. The diffraction pattern was indexed by a tetragonal unit cell [a and c respectively 11.6896(2) and 9.2357(3) A; M(20) = 195 and F(30) = 302; Z(calc… CONTINUE READING
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