Bromination of 1-Hydroxyimidazoles. Synthesis and Crystal Structures

  • Gerhard Lausa, Klaus Wursta, Volker Kahlenbergb, Herwig Schottenbergera
  • Published 2012

Abstract

Bromination of 1-hydroxyimidazole 3-oxide and 1-hydroxy-2-methylimidazole 3-oxide using bromine in acetic acid gave 2-bromo-1,3-dihydroxyimidazole hydrobromide and 4,5-dibromo-1,3-dihydroxy-2-methylimidazole hydrobromide, respectively. In contrast, bromination in aqueous mixture (acetic acid, methanol, dimethylformamide, tetrahydrofuran) yielded 2,4,5… (More)

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