Application of capillary electrophoresis with laser-induced fluorescence detection for the determination of trace neodymium in spent nuclear fuel using complexation with an emissive macrocyclic polyaminocarboxylate probe.

@article{Haraga2014ApplicationOC,
  title={Application of capillary electrophoresis with laser-induced fluorescence detection for the determination of trace neodymium in spent nuclear fuel using complexation with an emissive macrocyclic polyaminocarboxylate probe.},
  author={Tomoko Haraga and Shingo Saito and Yoshiyuki Sato and Shiho Asai and Yukiko Hanzawa and Hitoshi Hoshino and Masami Shibukawa and Ken-ichiro Ishimori and Kuniaki Takahashi},
  journal={Analytical sciences : the international journal of the Japan Society for Analytical Chemistry},
  year={2014},
  volume={30 7},
  pages={773-6}
}
A simple and rapid method with low radiation exposure risk was developed for the determination of neodymium in spent nuclear fuel by capillary electrophoresis with laser-induced fluorescence detection using a fluorescent probe having a macrocyclic hexadentate polyaminocarboxylate structure. The concentration of Nd(III) in a spent nuclear fuel sample was determined with no interference from various matrix elements, including lanthanides and uranium (at a 200-fold excess), with 92 ± 3% recovery… CONTINUE READING
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