Analysis of trace-level nitrated polycyclic aromatic hydrocarbons in water samples by solid-phase microextraction with gas chromatography and mass spectrometry.

A solid-phase microextraction coupled with gas chromatography and mass spectrometry method has been developed for the determination of ten nitrated polycyclic aromatic hydrocarbons in water samples. Five different kinds of commerical fibers were used to compare the extraction efficiency, including 65 μm polydimethylsiloxane/divinylbenzene, 100 μm… (More)