Analysis of psilocybin and psilocin in Psilocybe subcubensis Guzmán by ion mobility spectrometry and gas chromatography-mass spectrometry.

@article{Keller1999AnalysisOP,
  title={Analysis of psilocybin and psilocin in Psilocybe subcubensis Guzm{\'a}n by ion mobility spectrometry and gas chromatography-mass spectrometry.},
  author={Tomasz Keller and Aurore Schneider and Priska Regenscheit and Richard Dirnhofer and Thomas R{\"u}cker and J{\"u}rgen Jaspers and Wolfgang Kisser},
  journal={Forensic science international},
  year={1999},
  volume={99 2},
  pages={93-105}
}
A new method has been developed for the rapid analysis of psilocybin and/or psilocin in fungus material using ion mobility spectrometry. Quantitative analysis was performed by gas chromatography-mass spectrometry after a simple one-step extraction involving homogenization of the dried fruit bodies of fungi in chloroform and derivatization with MSTFA. The proposed methods resulted in rapid procedures useful in analyzing psychotropic fungi for psilocybin and psilocin. 
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