Analysis of pesticide residues in essential oils of citrus fruit by GC-MS and HPLC-MS after solid-phase extraction.

@article{Barrek2003AnalysisOP,
  title={Analysis of pesticide residues in essential oils of citrus fruit by GC-MS and HPLC-MS after solid-phase extraction.},
  author={Sami Barrek and Olivier Paisse and Marie-Florence Grenier-Loustalot},
  journal={Analytical and bioanalytical chemistry},
  year={2003},
  volume={376 2},
  pages={157-61}
}
A robust reliable method for the analysis of residues of pesticides in citrus groves was developed. Residues of twelve pesticides were extracted from citrus essential oils by SPE, separated by liquid chromatography and analyzed by GC-MS. In addition, ten pesticides were extracted by SPE, separated and analyzed by electrospray HPLC-MS. In the case of lemon essential oils, all twenty residues were separated by liquid/solid extraction on a mixed Florisil-C(18) cartridge. The method enabled the… CONTINUE READING

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