Analysis of perfluorinated carboxylic acids in soils II: optimization of chromatography and extraction.

@article{Washington2008AnalysisOP,
  title={Analysis of perfluorinated carboxylic acids in soils II: optimization of chromatography and extraction.},
  author={John W. Washington and W. Matthew Henderson and J Jackson Ellington and Thomas M. Jenkins and John J. Evans},
  journal={Journal of chromatography. A},
  year={2008},
  volume={1181 1-2},
  pages={21-32}
}
With the objective of detecting and quantitating low concentrations of perfluorinated carboxylic acids (PFCAs), including perfluorooctanoic acid (PFOA), in soils, we compared the analytical suitability of liquid chromatography columns containing three different stationary phases, two different liquid chromatography-tandem mass spectrometry (LC/MS/MS) systems, and eight combinations of sample-extract pretreatments, extractions and cleanups on three test soils. For the columns and systems we… CONTINUE READING
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