Analysis of 17 polar to semi-polar pesticides in the Ebro river delta during the main growing season of rice by automated on-line solid-phase extraction-liquid chromatography-tandem mass spectrometry.

@article{Kuster2008AnalysisO1,
  title={Analysis of 17 polar to semi-polar pesticides in the Ebro river delta during the main growing season of rice by automated on-line solid-phase extraction-liquid chromatography-tandem mass spectrometry.},
  author={Marina Kuster and Mar{\'i}a Jos{\'e} L{\'o}pez de Alda and Carlos Barata and Demetrio Rald{\'u}a and Dami{\'a} Barcel{\'o}},
  journal={Talanta},
  year={2008},
  volume={75 2},
  pages={390-401}
}
This work describes the optimization of a fully automated method based on on-line solid-phase extraction-liquid chromatography-electrospray-tandem mass spectrometry (SPE-LC-ESI-MS/MS) for the simultaneous determination of 17 medium to polar pesticides in water. The list of target analytes included organophosphates, triazines, phenylureas, anilides, chloroacetanilides, acidic herbicides and thiocarbamates. Detection limits achieved were below 5 ng/L for all compounds except metolachlor (12 ng/L… CONTINUE READING

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