An efficient method for the determination of enantiomeric purity of racemic amino acids using micellar chromatography, a green approach.

@article{Alwera2020AnEM,
  title={An efficient method for the determination of enantiomeric purity of racemic amino acids using micellar chromatography, a green approach.},
  author={Shiv Alwera and Vijay Alwera and Suman Sehlangia},
  journal={Biomedical chromatography : BMC},
  year={2020},
  pages={
          e4943
        }
}
  • Shiv Alwera, Vijay Alwera, Suman Sehlangia
  • Published 2020
  • Chemistry, Medicine
  • Biomedical chromatography : BMC
    • A simple, sensitive and green micellar liquid chromatographic method (RP-HPLC) was developed for enantioseparation of four racemic amino acids, namely, (RS)-selenomethionine, (RS)-methionine, (RS)-cysteine and (RS)-penicillamine. The aqueous solution of sodium dodecyl sulphate and Brij-35 was prepared and used as mobile phase for HPLC analysis. Activated esters of (S)-ibuprofen, (S)-ketoprofen, and (S)-levofloxacin were synthesized by reacting them with N-hydroxybenzotriazole. These esters were… CONTINUE READING
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    References

    SHOWING 1-10 OF 29 REFERENCES
    In Situ Derivatization of (RS)-Mexiletine and Enantioseparation Using Micellar Liquid Chromatography: A Green Approach
    • 3
    RP-HPLC enantioseparation of β-adrenolytics using micellar mobile phase without organic solvents.
    • 4
    (RS)-Propranolol: enantioseparation by HPLC using newly synthesized (S)-levofloxacin-based reagent, absolute configuration of diastereomers and recovery of native enantiomers by detagging.
    • 15
    Liquid chromatographic enantioseparation of three beta-adrenolytics using new derivatizing reagents synthesized from (S)-ketoprofen and confirmation of configuration of diastereomers.
    • 9
    Micellar liquid chromatography for the determination of drug materials in pharmaceutical preparations and biological samples
    • 105
    Reversed-phase liquid chromatography with mixed micellar mobile phases of Brij-35 and sodium dodecyl sulphate: a method for the analysis of basic compounds
    • 25
    A concise review of applications of micellar liquid chromatography to study biologically active compounds.
    • 11
    Model for micellar effects on liquid chromatography capacity factors and for determination of micelle-solute equilibrium constants
    • 209
    Greening analytical chromatography
    • 187
    • PDF
    N‐Hydroxyverbindungen als Katalysatoren für die Aminolyse aktivierter Ester
    • 129