A simple method for the simultaneous determination of mushroom toxins by liquid chromatography–time-of-flight mass spectrometry

@article{Yoshioka2013ASM,
  title={A simple method for the simultaneous determination of mushroom toxins by liquid chromatography–time-of-flight mass spectrometry},
  author={Naoki Yoshioka and Shigeki Akamatsu and Takao Mitsuhashi and Chikage Todo and Minoru Asano and Yasuhiro Ueno},
  journal={Forensic Toxicology},
  year={2013},
  volume={32},
  pages={89-96}
}
A simple and rapid method for the determination of nine mushroom toxins, ibotenic acid, propargylglycine, choline, muscimol, muscarine, α-amanitin, β-amanitin, phalloidin, and phallacidin, in mushroom samples has been developed. Mushroom toxins were extracted with 0.5 % formic acid in methanol/water, purified with Oasis HLB cartridges, and analyzed by liquid chromatography–time-of-flight mass spectrometry. The separation was performed on a pentafluorophenylpropyl column, and the mass… CONTINUE READING

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