A second monoclinic polymorph of 1-benzyl-N-methyl-1H-pyrrole-2-carboxamide


In the title compound, C(13)H(14)N(2)O, the N(pyrrole)-C(H(2))-C-C torsion angle is -7.7 (3)° and the dihedral angle between the pyrrole and benzene rings is 83.6 (2)°. In the crystal, inter-molecular N-H⋯O hydrogen bonds link the mol-ecules into chains extending along the c axis. We have previously reported another polymorphic form of this title compound, which has the same space group with different cell parameters: a = 9.8285 (18) Å, b = 23.588 (4) Å, c = 9.9230 (17) Å, β = 90.107 (3)°, Z = 8 and V = 2300.5 (7) Å(3) [Zeng et al. (2010 ▶). Acta Cryst. E66, o2051].

DOI: 10.1107/S1600536811030364

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@inproceedings{Wang2011ASM, title={A second monoclinic polymorph of 1-benzyl-N-methyl-1H-pyrrole-2-carboxamide}, author={Chang Jun Wang and Xiang Chao Zeng and Shi Hai Xu}, booktitle={Acta crystallographica. Section E, Structure reports online}, year={2011} }