A novel vic-dioxime ligand and its Ni(II), Cu(II) and Co(II) complexes containing calix[4]pyrrole moiety: synthesis, characterization and redox properties

@article{Taner2012ANV,
  title={A novel vic-dioxime ligand and its Ni(II), Cu(II) and Co(II) complexes containing calix[4]pyrrole moiety: synthesis, characterization and redox properties},
  author={Bilge Taner and Pervin Deveci and Emine {\"O}zge {\"O}zcan and Ali Osman Solak},
  journal={Journal of Inclusion Phenomena and Macrocyclic Chemistry},
  year={2012},
  volume={74},
  pages={391-396}
}
A new calix[4]pyrrole functionalized vic-dioxime, 3-(4-methyl-9,9,14,14,19,19-hexaethylcalix[4]pyrrole)benzoaminoglyoxime (LH2) was synthesized from anti-chloroglyoxime and 3-aminophenyl-calix[4]pyrrole at room temperature. The mononuclear complexes {nickel(II), copper(II) and cobalt(II)} of this vic-dioxime ligand were prepared and their structures were confirmed by elemental analysis, IR and UV–Vis spectrophotometry, magnetic susceptibility; the MS, 1H and 13C NMR spectra of the LH2 ligand… CONTINUE READING

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