A new NMR method for directly monitoring and quantifying the dissolution kinetics of starch in DMSO.

@article{Dona2007ANN,
  title={A new NMR method for directly monitoring and quantifying the dissolution kinetics of starch in DMSO.},
  author={Anthony Dona and Chun-Wai Wayne Yuen and Jonathan Peate and Robert G Gilbert and Patrice Castignolles and Marianne Gaborieau},
  journal={Carbohydrate research},
  year={2007},
  volume={342 17},
  pages={2604-10}
}
The kinetics of dissolution of starch is needed for (i) understanding digestive processes; (ii) providing data that could correlate with higher levels of starch structure; (iii) improving techniques for starch characterization in solution. A novel method is presented here to directly monitor these dissolution kinetics by time-resolved (1)H solution-state nuclear magnetic resonance (NMR); studies were carried out in deuterated dimethyl sulfoxide (DMSO-d(6)). By assuming pseudo-first-order… CONTINUE READING

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