A combined solid-state NMR and X-ray crystallography study of the bromide ion environments in triphenylphosphonium bromides.

Abstract

Multinuclear ((31)P and (79/81)Br), multifield (9.4, 11.75, and 21.1 T) solid-state nuclear magnetic resonance experiments are performed for seven phosphonium bromides bearing the triphenylphosphonium cation, a molecular scaffold found in many applications in chemistry. This is undertaken to fully characterise their bromine electric field gradient (EFG… (More)
DOI: 10.1002/chem.201103478

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