A SEC-HPLC-ICP MS hyphenated technique for identification of sulfur-containing arsenic metabolites in biological samples.

@article{Mandal2008ASM,
  title={A SEC-HPLC-ICP MS hyphenated technique for identification of sulfur-containing arsenic metabolites in biological samples.},
  author={Badal kumar Mandal and Kazuo T. Suzuki and Kazunori Anzai and Kentaro Yamaguchi and Yoshihisa Sei},
  journal={Journal of chromatography. B, Analytical technologies in the biomedical and life sciences},
  year={2008},
  volume={874 1-2},
  pages={64-76}
}
The present study describes the synthesis and characterization of thioarsenicals using electro-spray ionization-MS and time of flight-MS. Separation of thioarsenicals was found to be better by size-exclusion column compared to anion exchange column coupled with HPLC-inductively coupled argon plasma mass spectrometer (ICP MS). Although four thioarsenicals were confirmed as dimethylthioarsinous acid (m/z=138), methylmonothioarsonous acid (m/z=122), dimethyldithioarsinic acid (m/z=170) and… CONTINUE READING

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References

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Showing 1-4 of 4 references

Environ

M. Styblo, Z. Drobna, I. Jaspers, S. Lin, D. J. Thomas
Health Perspect. 110 (Suppl. 5) • 2002
View 1 Excerpt

Toxicol

L. Vega, M. Styblo, +3 authors D. Germolec
Appl. Pharmacol. 172 • 2001

Arch

M. Styblo, L. M. Del Razo, +7 authors D. J. Thomas
Toxicol. 74 • 2000

Chem

W. R. Cullen, K. J. Reimer
Rev. 89 • 1989
View 1 Excerpt

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