9-Fluoreneacetyl-tagged, solid-phase reagent for derivatization in direct plasma injection.

@article{Zhou19929FluoreneacetyltaggedSR,
  title={9-Fluoreneacetyl-tagged, solid-phase reagent for derivatization in direct plasma injection.},
  author={F. Zhou and I. Krull and B. Feibush},
  journal={Journal of chromatography},
  year={1992},
  volume={609 1-2},
  pages={
          103-12
        }
}
  • F. Zhou, I. Krull, B. Feibush
  • Published 1992
  • Chemistry, Medicine
  • Journal of chromatography
  • We describe here a resin-based derivatization reagent, containing a 9-fluoreneacetyl tag on a controlled-pore substrate, for direct injection analysis of amphetamine in plasma. On-line, pre-column derivatization was performed by direction injection of diluted plasma sample into an sodium dodecyl sulfate-containing mobile phase. Amphetamine was trapped in the hydrophobic derivatization column and derivatized at elevated temperature by the activated solid-phase reagent. The derivatized 9… CONTINUE READING
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