1H-1H MAS correlation spectroscopy and distance measurements in a deuterated peptide.

@article{Reif20011H1HMC,
  title={1H-1H MAS correlation spectroscopy and distance measurements in a deuterated peptide.},
  author={Bernd Reif and Christopher P Jaroniec and Chad M Rienstra and Morten Hohwy and Robert G Griffin},
  journal={Journal of magnetic resonance},
  year={2001},
  volume={151 2},
  pages={
          320-7
        }
}
In this Communication, we demonstrate the use of deuteration together with back substitution of exchangeable protons as a means of attenuating the strong 1H-1H couplings that broaden 1H magic angle spinning (MAS) spectra of solids. The approach facilitates 15N-1H correlation experiments as well as experiments for the measurement of 1H-1H distances. The distance measurement relies on the excellent resolution in the 1H MAS spectrum and homonuclear double quantum recoupling techniques. The 1H-1H… CONTINUE READING
Highly Cited
This paper has 74 citations. REVIEW CITATIONS

From This Paper

Figures, tables, and topics from this paper.

Citations

Publications citing this paper.
Showing 1-10 of 35 extracted citations

Applications of solid-state NMR to membrane proteins.

Biochimica et biophysica acta. Proteins and proteomics • 2017

74 Citations

0510'02'05'09'13'17
Citations per Year
Semantic Scholar estimates that this publication has 74 citations based on the available data.

See our FAQ for additional information.

References

Publications referenced by this paper.
Showing 1-10 of 57 references

Accurate C– 15N distance measurements in uniformly 13C, 15N-labeled peptides, J

C. P. Jaroniec, B. A. Tounge, J. Herzfeld, R. G. Griffin, Freque 13 selective heteronuclear dipolar recoupling in r solids
Am. Chem. Soc. 123,3507–3519 • 2001

Structures of two model p tides : N - acetyl - D , L - valine and N - acetyl - L - valyl - L - leucine

P. L. Stewart, S. J. Opella
J . Am . Chem . Soc . • 2001

A simple model for hetero clear spin decoupling in solid-state NMR

M. Ernst, H. Zimmermann, B. H. Meier
Chem. Phys. Lett • 2000

Chemical shift correla spectroscopy in rotating solids : Radio - frequency dipolar recoupling longitudinal exchange

J. H. Ok Bennett, R. G. Griffin, S. Vega
Chem . Phys . Lett . • 2000

D termination of the complete structure of a uniformly labeled molecule rotational resonance solid - state NMR in the tilted rotating frame

K. Takegoshi Nomura, T. Terao, K. Uchida, M. Kainosho
J . Am . Chem . Soc . • 2000

New approach to resolution proton NMR in solids : Deuterium spin decoupling by multi quantum transitions

D. J. Ruben Pines, S. Vega, M. Mehring
J . Magn . Reson . • 2000

Oschkina Sample optimization and identification of signal patterns of amino acid chains in 2D-RFDR spectra of the α-spectrin

J. Pauli, B. vanRossum, H. F ̈ orster, H.J.M. deGroot
J. Magn. Reson • 2000

Sample optimization and identification of signal patterns of amino acid chains in 2 D - RFDR spectra of the α - spectrin SH 3 domain

B. vanRossum Pauli, H. F ̈ orster, H. J. M. deGroot, H. Oschkina
J . Biomol . NMR • 2000