[Determination of primary aromatic amines in crayons gas chromatography-mass spectrometry].


A method for the determination of nine primary aromatic amines in crayon by solid phase extraction (SPE) and gas chromatography-mass spectrometry (GC-MS) was developed. The alkanes in the sample were removed with n-hexane. Then the sample was extracted twice with ultrasonic extraction by methanol. The extract was evaporated, then the concentrated solution… (More)