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OBJECTIVE To investigate the levels and influencing factors of phthalate internal exposure in pregnant women (gestation age ≤ 16 weeks). METHODS During April to June in 2013, 1 020 pregnant women (gestation age ≤ 16 weeks) who had established the maternal care manual were recruited in maternal and child health hospital of Siming District, Xiamen city.(More)
A method for the determination and analysis of tetrodotoxin (TTX) in nassarius using liquid chromatography-mass spectrometry (LC-MS) has been developed. The homogenized sample was extracted with 0.03 mol/L acetic acid by heating in a boiling water-bath for 10 min and then was cleaned up on a Sep-Pak C18 cartridge column and filtered through a M(r) 3 000(More)
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