Wolfgang Malisch

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The mu2-silylene-bridged iron complexes [Cp(OC)(2)Fe](2)SiX(2) (X = F (2), Br (4), I (5)) have been prepared from the mu2-SiH(2) functional precursor [Cp(OC)(2)Fe](2)SiH(2) (1) by hydrogen/halogen exchange, using HBF(4), CBr(4), and CH(2)I(2), respectively. The fluoro- and bromo-substituted derivatives 2 and 4 are converted upon UV irradiation to the(More)
The zwitterionic compounds Im-E-Mel [9, E S (a), Se (b), Te (c), Im 2-{1,3-diisopropyl-4,5-dimethylimidazolium}, Mel 5-{2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-ylide}] are obtained from the corresponding 2-chalcogeno-1,3-diisopropyl-4,5-dimethylimidazolines 8 and 5-bromo-2,2-dimethyl-4,6-dioxo-1,3-dioxan (7) in the presence of triethylamine in excellent yields.(More)
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