William B Motherwell

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Easy as 1,2,3: Reaction of methyl carbamate, triethyl orthoformate, and readily available alkenes provides a highly practical preparation of protected aminocyclopropanes. The reaction proceeds with preferential cis addition to alkenes, and cleavage of the methyl carbamate gives the free aminocyclopropanes as their HI salts.
Selective examples of OH...arene, NH2...arene and C-HN[triple bond, length as m-dash]C weak interactions are presented using a flexible dibenzobicyclo[3.2.2]nonane scaffold for detection and comparative characterisation of non-covalent interactions in solution and solid states.
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