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The aromatic electrophilic formylation reaction of azacalixarenepyridine and azacalixpyridine were systematically studied. By simply controlling the ratio of reactants and the reaction temperature, the Vilsmeier-Haack reaction selectively afforded mono-, di-, and tetra-formylated azacalixarenepyridines and azacalixpyridines. The… (More)
The synthesis, structure, and fullerene complexation property of novel and functionalized On-corona[n]arenes were reported. Based on the fragment coupling strategy, ester-containing On-corona[n]arenes (n = 6, 8) were obtained readily starting from 1,4-hydroquinone and diethyl 2,5-difluoroterephthalate. Reduction of esters with LiAlH4 produced almost… (More)