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The asymmetric unit of the title compound, C(10)H(18)N(2)O(6), contains two halves of two independent centrosymmetric mol-ecules with almost identical conformations. Weak inter-molecular C-H⋯O hydrogen bonds consolidate the crystal packing.
The asymmetric unit of the title compound, C(4)H(8)N(2)O(4), contains one half-mol-ecule which is completed via a crystallographic inversion centre. In the crystal structure, mol-ecules are arranged in undulating layers parallel to (001). Inter-molecular N-H⋯O and O-H⋯O hydrogen bonds consolidate this arrangement.
A new member of the polyazapolycyclic family of compounds, namely N(3),N(6),2,5,7-pentaphenyl-2,5,7-triazabicyclo[2.2.1]heptane-3,6-diamine xylene solvate, C(34)H(31)N(5).C(8)H(10), was synthesized for the first time and the crystal structure is reported. There are no hydrogen bonds joining the molecules. All four chiral C atoms have the same absolute… (More)
The title compound, C(48)H(43)N(7), is a polyaza-polycyclic compound with a near-C(2) symmetric skeleton. In the crystal, a N-H⋯π inter-action occurs.
Bruker (2005). APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA. Nielsen, A. T., Nissan, R. A., Cafin, A. P., Gilardi, R. D. & Gorge, C. F. (1992). J. Org. Chem. 57, 6756–6759. Nielsen, A. T., Nissan, R. A., Vanderah, D. J., Coon, C. L., Gilardi, R. D., George, C. F. & Anderson, J. F. (1990). J. Org. Chem. 55, 1459–1466. Nitravati, D. D. &… (More)
In the title compound, C(34)H(31)N(5), the observed molecular geometry suggests that anomeric effects are present in terms of short C-N bond lengths and reduced pyramidality of the N atoms.