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Eco-friendly synthesis of 5-hydroxymethylfurfural (HMF) and its application to the Ferrier-rearrangement reaction
ABSTRACT 5-Hydroxymethylfurfural was conveniently synthesized by dehydration of D-fructose in a good yield. To further build bioactive derivatives from 5-hydroxymethylfurfural, 2,3-unsaturatedExpand
TMSOTf mediated stereoselective synthesis of α-C-glycosides from unactivated aryl acetylenes
A metal free and highly stereoselective procedure for the synthesis of 2,3-unsaturated-C-glycosides has been developed between glycals and unactivated aryl acetylenes in the presence of TMSOTfExpand
Ferric Chloride: An Eco-friendly Catalyst for the Stereoselective Synthesis of 2-Deoxy Aryl-O-Rhamnosides
A facile and direct O -glycosylation method for the stereoselective synthesis of 2,6-dideoxy α- O -aryl-glycosides has been described using an eco-friendly catalyst, ferric chloride (FeCl 3 ). TheExpand
Substoichiometric FeCl3 Activation of Propargyl Glycosides for the Synthesis of Disaccharides and Glycoconjugates
Glycosides as glycosyl donors using FeCl3 have been described. Under optimal reaction conditions, three kinds of propargyl glycosides were found to react with steroids and sugar-derived glycosylExpand
A Facile and Direct Glycosidation Method for the Synthesis of 2-Deoxy α-Rhamnosides Catalyzed by Ferric Chloride
A facile and highly efficient O-glycosylation method for stereoselective synthesis of 2,6-dideoxy-O-glycosides has been described promoted by FeCl3, an eco-friendly, easily available and non-toxicExpand
A Highly Efficient Magnetic Iron(III) Nanocatalyst for Ferrier Rearrangements
A novel and highly efficient magnetic Fe3O4@C@Fe(III) core–shell catalyst, in which the carbon shell was prepared from lotus leaf, was fabricated. This nanocatalyst was successfully applied in theExpand
Magnetic Core-Shell Fe3O4@C-SO3H as an Efficient and Renewable ‘Green Catalyst’ for the Synthesis of O-2,3-Unsaturated Glycopyranosides
A magnetic core-shell solid-acid catalyst Fe3O4@C-SO3H was studied for synthesis of O-2,3-unsaturated glycosides through Ferrier rearrangement. The donors include 3,4,6-tri-O-acetyl- d -glucal andExpand
Study on the Chemical Integrated and Designing Experiment Course of Undergraduate
According to the current situation of integrated and designing experiments in our college, experiments involving the extract, identification and determination of polysaccharides and flavonoids inExpand