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Efficient one-pot synthesis of 5-ethoxymethylfurfural from fructose catalyzed by heteropolyacid supported on K-10 clay
Abstract Synthesis of 5-ethoxymethylfurfural (EMF) from the etherification of 5-hydroxymethylfurfural (HMF) and the dehydrative etherification of fructose over K-10 clay supportedExpand
Studies toward asymmetric synthesis of leiodelide A
An enantioselective route for oxazoline 4, a key fragment toward the asymmetric synthesis of leiodelide A, is described. We synthesized northern subunit 6 through a Julia–Lythgoe olefination andExpand
A flexible approach to construct three contiguous chiral centers of sphingolipids, and asymmetric synthesis of d-ribo-phytosphingosine and its derivatives
Abstract An efficient approach to build the three contiguous stereogenic centers of sphingosine unit starting from cheap glutamic acid is described. The key step of this approach is the SmI 2Expand
Diverse synthesis of marine cyclic depsipeptide lagunamide A and its analogues.
The asymmetric total synthesis of lagunamide A and its five analogues and itsFive analogues, including the structure dehydrated at the C37 position, and the C7 configuration dramatically affected the ring closure are detailed in this report. Expand
Asymmetric synthesis of emericellamide B
Asymmetric total synthesis of emericellamide B (9.4%, 17 longest linear steps) is detailed in this report. In this synthetic route, the highly methylatedExpand
Flexible approach for the asymmetric synthesis of (−)-hyacinthacine A1 and its 7a-epimer
Abstract The diastereoselective nucleophilic addition of organic boronic ester to 3-hydroxy-2-substituted N -acyliminium ions 9 led to the formation of 2,5- cis -pyrrolidine 10 , from which aExpand
Novel 3,4-dihydropyrimidinones modified with N3-alkyloxymethyl, aminomethyl, arylsulfonylmethyl, and azidomethyl groups can be regioselectively obtained over their isomeric N1 compounds in goodExpand
N-Alkoxymethylation of heterocyclic compounds with diethyl phosphite via cleavage of P–O bond
Abstract N -Alkoxymethylation of heterocyclic compounds with diethyl phosphite via cleavage of P–O bond was investigated and a series of N 3-ethoxymethylated heterocyclic compounds were synthesized.Expand
Synthesis of 2-Substituted Pyrimidines via Cross-Coupling Reaction of Pyrimidin-2-yl Sulfonates with Nucleophiles in Polyethylene Glycol 400
A mild and rapid procedure to the synthesis of 2-substituted pyrimidines was developed via sequential functionalization of easily available Biginelli 3,4-dihydropyrimidine-2(1H)-ones via oxidation,Expand