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Multi-mycotoxin analysis in eggs using a QuEChERS-based extraction procedure and ultra-high-pressure liquid chromatography coupled to triple quadrupole mass spectrometry.
TLDR
UHPLC-MS/MS coupled to tandem mass spectrometry has been used for the analysis of these compounds in less than 7 min and aflatoxins B1, B2, G1, G2, and beauvericin were detected at trace levels. Expand
Comparison of several extraction techniques for multiclass analysis of veterinary drugs in eggs using ultra-high pressure liquid chromatography-tandem mass spectrometry.
TLDR
This study compared four extraction methods for the simultaneous determination of tetracyclines, macrolides, quinolones, sulphonamides and anthelmintics in eggs by ultra-high pressure liquid chromatography coupled to tandem mass spectrometry (UHPLC-MS/MS). Expand
Development and validation of a multiclass method for the determination of veterinary drug residues in chicken by ultra high performance liquid chromatography-tandem mass spectrometry.
A multiclass method has been optimized and validated for the simultaneous determination of 20 veterinary drug residues belonging to several classes, as quinolones, sulfonamides, macrolides,Expand
Simple and high-throughput method for the multimycotoxin analysis in cereals and related foods by ultra-high performance liquid chromatography/tandem mass spectrometry
Abstract A rapid, reliable and sensitive method was developed to determine 12 mycotoxins (deoxynivalenol, aflatoxins B1, B2, G1, G2 and M1, fumonisins B1 and B2, ochratoxin A, HT-2 and T-2 toxin andExpand
Multiresidue determination of veterinary drugs in aquaculture fish samples by ultra high performance liquid chromatography coupled to tandem mass spectrometry.
A simple, selective and fast multiresidue method was developed for the determination of 32 veterinary drug residues belonging to several families, in gilthead sea bream (Sparus aurata) by ultra highExpand
Multiresidue method for fast determination of pesticides in fruit juices by ultra performance liquid chromatography coupled to tandem mass spectrometry.
A new analytical method for the simultaneous determination of 90 pesticides in fruit juices by ultra performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS) has beenExpand
Application of conventional solid-phase extraction for multimycotoxin analysis in beers by ultrahigh-performance liquid chromatography-tandem mass spectrometry.
TLDR
This methodology combines the simplicity of SPE using conventional cartridges and UHPLC-MS/MS, producing a rapid, sensitive, and reliable procedure. Expand
Multi-class methodology to determine pesticides and mycotoxins in green tea and royal jelly supplements by liquid chromatography coupled to Orbitrap high resolution mass spectrometry.
TLDR
A multi-class methodology was developed to determine pesticides and mycotoxins in food supplements, and the best results were obtained using C18 and zirconium oxide for green tea and royal jelly, respectively. Expand
Comparison of the efficiency of different extraction methods for the simultaneous determination of mycotoxins and pesticides in milk samples by ultra high-performance liquid chromatography-tandem
A rapid multi-analyte method has been developed for the simultaneous determination of pesticides and mycotoxins in milk by ultra high-performance liquid chromatography coupled to triple quadrupoleExpand
Analysis and study of the distribution of polar and non-polar pesticides in wastewater effluents from modern and conventional treatments.
TLDR
The proposed methodologies involved the determination of 39 polar and 139 non-polar pesticides using solid-phase extraction (SPE) and pressurized-liquid extraction (PLE) for the extraction of the aqueous phase and the SPM, respectively. Expand
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