A novel chemiluminescence (CL) reaction, thiosemicarbazide (TSC)-H(2)O(2), for the determination of copper at nanogram per milliliter level in batch type is described. The method is based on the… (More)
Partial least-squares (PLS) calibration and principal component regression (PCR) methods were utilized for the simultaneous spectrofluorimetric and spectrophotometric determination of pyridoxine (PY)… (More)
A highly sensitive spectrophotometric method is described for the determination of trace amounts of osmium(VIII), based on its catalytic effect on the oxidation of carminic acid by hydrogen peroxide.… (More)
A simple and convenient method has been developed for the speciation of chromium(III) and chromium(VI) in aqueous solutions using a sodium dodecyl sulphate coated alumina micro-column (1.5 cm x 5 mm… (More)
Periodic acid and its salts have been widely used for the quantitative oxidation of vic-diol containing compounds including carbohydrates and catecholamine drugs. The advantage of using a polymeric… (More)
Oscillating chemical reactions are complex systems, involving a large number of chemical species. In an oscillating chemical reaction, some species, usually a reaction intermediate, exhibit… (More)
A novel spectrophotometric method is described for the determination of epinephrine (EP) and norepinephrine (NE). The method is based on the development of a red colour with sodium bismuthate, as a… (More)
In this paper, oscillating chemiluminescence (CL), 1,10-phenanthroline H2O2-KSCN-CuSO4-NaOH system, was studied in a batch reactor. The system described is a novel, slowly damped oscillating CL… (More)
This paper describes simple and rapid methods for the fabrication of glass and polymeric chips for routine analytical applications. The methods are easily interfaced to the general laboratory… (More)
A simple and highly sensitive chemiluminescence (CL) method is reported for the determination of naphazoline hydrochloride (NH). It was found that the weak CL from the reaction of luminol and KIO4 in… (More)