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Validation according to European Commission Decision 2002/657/EC of a confirmatory method for aflatoxin M1 in milk based on immunoaffinity columns and high performance liquid chromatography with…
Survey of benzoic acid in cheeses: contribution to the estimation of an admissible maximum limit
- M. Iammarino, Aurelia Di Taranto, C. Palermo, M. Muscarella
- Chemistry, MedicineFood Additives & Contaminants, Part B
- 12 October 2011
Taking into account the distribution of benzoic acid concentrations observed in “positive” samples, it is plausible to estimate a maximum admissible limit of 40.0 mg kg−1 for benzoal acid in cheese, and samples can be considered “compliant”.
Survey of histamine levels in fresh fish and fish products collected in Puglia (Italy) by ELISA and HPLC with fluorimetric detection
Validation and application of multi-residue analysis of eight anticoagulant rodenticides by high-performance liquid chromatography with fluorimetric detection
- A. Armentano, M. Iammarino, S. L. Magro, M. Muscarella
- ChemistryJournal of veterinary diagnostic investigation…
- 1 March 2012
Validation and applications of a rapid and reliable method for the simultaneous determination of 8 anticoagulant rodenticides in baits and animal livers using high-performance liquid chromatography with fluorescence detection demonstrate suitability for application in official analysis and for monitoring purposes of animal poisoning by antICOagulants.
Determination of deoxynivalenol and nivalenol by liquid chromatography and fluorimetric detection with on-line chemical post-column derivatization.
Validation of a confirmatory analytical method for the determination of aflatoxins B1, B2, G1 and G2 in foods and feed materials by HPLC with on-line photochemical derivatization and fluorescence…
- M. Muscarella, M. Iammarino, D. Palermo
- Chemistry, MedicineFood additives & contaminants. Part A, Chemistry…
- 9 September 2009
The procedure for the determination of aflatoxins in food samples and cereals for animal consumption was extensively validated following Regulation (EC) No. 882/2004 and satisfies the necessary requirements for sensitivity, linearity, selectivity, precision and ruggedness.
Technical note: Rapid method for determination of amino acids in milk.
- R. Marino, M. Iammarino, A. Santillo, M. Muscarella, M. Caroprese, M. Albenzio
- Chemistry, MedicineJournal of dairy science
- 1 June 2010
A rapid method for measurement of amino acids in milk was developed and validated, characterized by high precision, low repeatability uncertainty, and high accuracy for all amino acids evaluated.
Sarcoidosis in an Italian province. Prevalence and environmental risk factors
The bioaccumulation analysis was an effective method to identify the mineral particles that mostly contribute to air pollution in the different areas, but it was not sufficient to establish a clear correlation between the onset of sarcoidosis and environmental risk factors.
A multiresidual method based on ion-exchange chromatography with conductivity detection for the determination of biogenic amines in food and beverages
- C. Palermo, M. Muscarella, D. Nardiello, M. Iammarino, D. Centonze
- Chemistry, MedicineAnalytical and Bioanalytical Chemistry
A sensitive and accurate method by ion chromatography and conductimetric detection has been developed for the determination of biogenic amines in food samples at microgram per kilogram levels and a good repeatability was obtained with precision levels in the range 0.03–0.32 %.
Development of a new analytical method for the determination of fumonisins B1 and B2 in food products based on high performance liquid chromatography and fluorimetric detection with post-column…