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En Route to 2-(Cyclobuten-1-yl)-3-(trifluoromethyl)-1H-indole.
TLDR
Compound 1a is a key impurity of reverse transcriptase inhibitor efavirenz, an important anti-HIV/AIDS drug, and synthetic challenges, dead ends, and detours are discussed. Expand
Seasonal and spatial variations in the occurrence, mass loadings and removal of compounds of emerging concern in the Slovene aqueous environment and environmental risk assessment.
TLDR
A constructed wetland showed the lowest (0-80%) and most inconsistent removal efficiencies of CECs including caffeine, two UV-filters, two preservatives and two APIs compared to other treatment technologies. Expand
A way to avoid using precious metals: the application of high-surface activated carbon for the synthesis of isoindoles via the Diels-Alder reaction of 2H-pyran-2-ones.
TLDR
It is proven that the aromatization occurs via a hydrogen transfer from the cyclohexadiene intermediate to the maleimide derivative (therefore producing succinimides), facilitated by the active surface of the heterogeneous carbon-based catalyst. Expand
1 H-15 N HMBC NMR as a tool for rapid identification of isomeric azaindoles: The case of 5F-MDMB-P7AICA.
TLDR
A simple and efficient flow chart diagram applicable for a rapid nuclear magnetic resonance (NMR) identification and differentiation between azaindoles, 4, 5, 6, and 7-azaindole, which is a common structural motif of synthetic cannabinoids, is reported. Expand
Hydrogenation of Condensed Aromatic Compounds over Mesoporous Bifunctional Catalysts Following a Diels–Alder Adduct Pathway
Pt(0.5 wt %)‐Al‐SBA‐15 and Pt(0.5 wt %)‐Al‐MCM‐41 bifunctional catalysts were prepared by wet impregnation and investigated in the hydrogenation of anthracene and the hydrogenolysis/hydrogenation ofExpand
Regioselective Hydrolysis and Transesterification of Dimethyl 3-Benzamidophthalates Assisted by a Neighboring Amide Group.
TLDR
An efficient, highly regioselective hydrolysis and transesterification of dimethyl 3-benzamidophthalates into the corresponding carboxylic acid monoesters and mixed esters under basic conditions is presented. Expand
Chloranil as an Efficient Oxidant of the Cyclohexadiene Intermediates Formed by a Cycloaddition of Substituted 2H‐Pyran‐2‐ones and Styrenes En Route to the Boscalid Derivatives
We describe a three-step one-pot metal-free domino procedure yielding a set of boscalid derivatives, parent compound being a highly important agrochemical agent. The first step of the processExpand