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The functionalised metal-organic framework MIL-101(Cr)-NH(2), containing 2-aminobenzene-1,4-dicarboxylate as the linker, has been synthesised. A new tandem post-synthetic modification strategy… Continue Reading
A series of new zinc-based metal-organic framework materials has been prepared in which deferiprone is incorporated as a chelating ligand on infinite or tri-zinc secondary building units following… Continue Reading
The synthesis, structural and thermal characterisation of a number of coordination complexes featuring the N,O-heteroditopic ligand 4-(3,5-dimethyl-1H-pyrazol-4-yl)benzoate, HL are reported. The… Continue Reading
The amine-functionalised metal–organic framework (MOF) [Zn4O(bdc-NH2)3] (IRMOF-3, bdc-NH2 = 2-amino-1,4-benzenedicarboxylate) has been post-synthetically modified in a tandem condensation-reduction… Continue Reading
The current status and technical details of the four instruments dedicated to X-ray spectroscopy available at Diamond Light Source are presented.
Post-synthetic modification (PSM) of metal-organic frameworks (MOFs) has increased in importance in the last decade, as a pathway to access more complex surfaces in the pores and channels of porous… Continue Reading
[Zn4O(bdc-NH2)3], IRMOF-3 (bdc-NH2 = 2-amino-1,4-benzenedicarboxylate), and [Cr3O(H2O)2F(bdc-NH2)3], MIL-101(Cr)-NH2, undergo tandem post-synthetic modification reactions with aldehydes and NaCNBH3… Continue Reading
Abstract The product from the reaction between Cd(NO 3 ) 2 ·4H 2 O and 1,3,5-benzenetricarboxylic acid (H 3 btc) in DMF at 95 °C depends on the reaction time, with [Cd(Hbtc)(H 2 O) 2 ] 1 and… Continue Reading
A scanning four-bounce monochromator that offers an unprecedented level of stability in the incident beam energy resolution and calibration has been developed for a flagship spectroscopy beamline at… Continue Reading
Small redox active molecules such as alizarin red S are readily adsorbed and bound into redox-inactive metal–organic framework hosts such as UMCM-1. Redox activity of the bound guest molecule is of… Continue Reading