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This study reports the development of a novel multiplug filtration cleanup (m-PFC) procedure for analysis of pesticide residues in leek samples followed by gas chromatography-tandem mass spectrometry detection. The leek samples were initially purified following the dispersive solid-phase extraction with different sorbents to determine the most suitable(More)
An analytical method based on dispersive solid-phase extraction with a multiwalled carbon nanotubes sorbent coupled with positive pulse glow discharge ion mobility spectrometry was developed for analysis of 30 pesticide residues in drinking water samples. Reduced ion mobilities and the mass-mobility correlation of 30 pesticides were measured. The pesticides(More)
Ochratoxin A (OTA) represents one of the most widespread mycotoxins in agricultural commodities in the world and is considered a possible human carcinogen with its potent nephrotoxicity. OTA is stable under most food processing conditions; however, higher-temperature treatment may reduce OTA content in foods. Since OTA can be found in processed products(More)
This study reports the development and validation of a novel rapid cleanup method based on multiple-walled carbon nanotubes in a packed column filtration procedure for analysis of pesticide residues followed by gas chromatography-triple-quadruple tandem mass spectrometry detection. The cleanup method was carried out by applying the streamlined procedure on(More)
A modified quick, easy, cheap, effective, rugged (QuEChERS) method with multi-walled carbon nanotubes (MWCNTs) as reversed-dispersive solid phase extraction (r-DSPE) material was applied to the analysis of pirimiphos-methyl and deltamethrin residues in stored rice. Two dustable powder (DP) formulations (2% pirimiphos-methyl and deltamethrin DP; 5%(More)
Uniconazole residue dynamics and final residues in supervised field trials at GAP conditions were studied. The residue levels and dissipation rate of uniconazole was detected by LC-MS. At fortification levels of 0.04, 0.2 and 2 mg kg(-1), recoveries ranged from 78.7 % to 100.9 % with RSDs of 0.1 %-4.6 % (n = 5). The dissipation experiments showed the(More)
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