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Direct observation of a borane-silane complex involved in frustrated Lewis-pair-mediated hydrosilylations.
Perfluorarylborane Lewis acids catalyse the addition of silicon-hydrogen bonds across C=C, C=N and C=O double bonds. This 'metal-free' hydrosilylation has been proposed to occur via borane activationExpand
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Mono- and Bis(imidazolidinium ethynyl) Cations and Reduction of the Latter To Give an Extended Bis-1,4-([3]Cumulene)-p-carboquinoid System.
An extended π-system containing two [3]cumulene fragments separated by a p-carboquinoid and stabilized by two capping N-heterocyclic carbenes (NHCs) has been prepared. Mono- and bis(imidazolidiniumExpand
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Intermolecular oxidative dehydrogenative 3,3′-coupling of benzo[b]furans and benzo[b]thiophenes promoted by DDQ/H+: total synthesis of shandougenine B
With an excess of a strong acid, 2,3-dichloro-5,6-dicyano-1,4-quinone (DDQ) is shown to promote metal-free intermolecular oxidative dehydrogenative (ODH) 3,3′-coupling of 2-aryl-benzo[b]furans andExpand
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Synthesis of new hybrid 1,4-thiazinyl-1,2,3-dithiazolyl radicals via Smiles rearrangement.
The condensation reaction of 2-aminobenzenethiols and 3-aminopyrazinethiols with 2-amino-6-fluoro-N-methylpyridinium triflate afforded thioether derivatives that were found to undergo SmilesExpand
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Synthesis and characterisation of p-block complexes of biquinoline at different ligand charge states.
The first examples of p-block coordination complexes of biquinoline, namely [(biq)BCl2]Cl and [(biq)BCl2]˙, were synthesized and structurally characterized. The acquired data allowed the estimationExpand
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Comment on "crystallographic snapshot of an arrested intermediate in the biomimetic activation of CO2 ".
Out of focus: A recent Communication published in this journal describes the synthesis of [nBu4 N]HCO3 . The authors performed a single-crystal X-ray study that revealed a putative species describedExpand
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CCDC 1519804: Experimental Crystal Structure Determination
Related Article: Petra Vasko, Juha Hurmalainen, Akseli Mansikkamaki, Anssi Peuronen, Aaron Mailman, Heikki M. Tuononen|2017|Dalton Trans.|46|16004|doi:10.1039/C7DT03243A
CCDC 1536800: Experimental Crystal Structure Determination
Related Article: Petra Vasko, Juha Hurmalainen, Akseli Mansikkamaki, Anssi Peuronen, Aaron Mailman, Heikki M. Tuononen|2017|Dalton Trans.|46|16004|doi:10.1039/C7DT03243A
CCDC 1519806: Experimental Crystal Structure Determination
Related Article: Petra Vasko, Juha Hurmalainen, Akseli Mansikkamaki, Anssi Peuronen, Aaron Mailman, Heikki M. Tuononen|2017|Dalton Trans.|46|16004|doi:10.1039/C7DT03243A
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