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Microwave-Assisted Synthesis of 1,3,4-Thiadiazole Schiff Base Derivatives
A rapid and efficient microwave-assisted synthesis method for the preparation of 1,3,4-thiadiazole Schiff base derivatives is described. These 1,3,4-thiadiazole Schiff bases (5a-h) were identified by…
Generation of synthetic equivalents of benzdiynes from benzobisoxadisiloles.
- Yali Chen, Jianguang Sun, Xin Wei, W. Wong, A. Lee
- ChemistryThe Journal of organic chemistry
- 14 September 2004
The synthesis of naphthoxadisilole 28, which can serve as the precursor of 2,3-naphthyne, is described and highly substituted arenes were obtained by removing the oxygen bridges from the furan adducts.
Synthesis of 3, 3-bis (difluoramino) octahydro-1, 5, 7, 7-tetranitro-1, 5-diazocine (TNFX, a diversified energetic heterocycle)
A Clerodane Diterpene with Antibacterial Activity from Ajuga lupulina.
Generation of Synthetic Equivalents of Benzdiynes from Benzobisoxadisiloles.
In the title compound, C10H18N2O4, the diazacyclohexane ring is in a normal chair conformation. The molecule packs to form hydrogen-bonded dimers around a center of symmetry.
Convenient Acylative Dealkylation of Tertiary Amines.
The conformation of the title compound, C15H28N4O4, was determined. The tricyclic nine-membered ring has a boat-shaped azacyclohexane ring on one side of the bridge and a chair-shaped ring on the…
The conformation and density were determined for the title compound, C7H10N6O8. As expected, the bicyclic nine-membered ring has two chair-shaped azacyclohexane rings.