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Microwave-Assisted Synthesis of 1,3,4-Thiadiazole Schiff Base Derivatives
A rapid and efficient microwave-assisted synthesis method for the preparation of 1,3,4-thiadiazole Schiff base derivatives is described. These 1,3,4-thiadiazole Schiff bases (5a-h) were identified by
Generation of synthetic equivalents of benzdiynes from benzobisoxadisiloles.
The synthesis of naphthoxadisilole 28, which can serve as the precursor of 2,3-naphthyne, is described and highly substituted arenes were obtained by removing the oxygen bridges from the furan adducts.
In the title compound, C10H18N2O4, the di­aza­cyclo­hexane ring is in a normal chair conformation. The mol­ecule packs to form hydrogen-bonded dimers around a center of symmetry.
The conformation of the title compound, C15H28N4O4, was determined. The tricyclic nine-membered ring has a boat-shaped aza­cyclo­hexane ring on one side of the bridge and a chair-shaped ring on the
The conformation and density were determined for the title compound, C7H10N6O8. As expected, the bicyclic nine-membered ring has two chair-shaped aza­cyclo­hexane rings.