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Total syntheses of tumor-related antigens N3: probing the feasibility limits of the glycal assembly method.
- H. M. Kim, I. J. Kim, S. Danishefsky
- ChemistryJournal of the American Chemical Society
- 10 January 2001
The total syntheses of two octasaccharide antigens isolated from human milk, 1 and 2, and their corresponding allyl glycosides, 3 and 4, have been achieved by utilizing the glycal method. Convergent…
Total Synthesis and Proof of Structure of a Human Breast Tumor (Globo‐ H) Antigen
Co2(CO)8-mediated endo mode cyclization of epoxy-alcohol: synthesis of 2-ethynyl-3-hydroxy-2-methyltetrahydropyran and 2-ethynyl-3-hydroxy-3-methyltetrahydropyran derivatives.
The preferential endo mode cyclization over the exo one was observed in these experiments and the tetrahydropyran derivatives with the cobalt-complexed moiety were provided.
Defining the Molecular Recognition of Globo H (Human Breast Cancer) Antigen Through Probe Structures Prepared by Total Synthesis.
Efficient Construction of 4‐Oxo‐1,3‐diazabicyclo(3.3.0)octanes via Thiohydantoins.
The First Successful Intramolecular Diels-Alder Reaction Leading to a Baccatin III Construct Bearing Oxygen Functionality at C10.