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Adsorption Kinetic and Thermodynamic Studies of Phosphate onto Tantalum Hydroxide
TLDR
Foreign anions tests showed that the presence of competitive ions cause minimal interference with the adsorption of phosphate on tantalum hydroxide.
Visible-light-promoted iminyl-radical formation from acyl oximes: a unified approach to pyridines, quinolines, and phenanthridines.
TLDR
A unified strategy involving visible-light-induced iminyl-radical formation has been established for the construction of pyridines, quinolines, and phenanthridines from acyl oximes and was successfully applied to a five-step concise synthesis of benzo[c]phenanthridine alkaloids.
Radical Alkynyltrifluoromethylation of Alkenes Initiated by an Electron Donor-Acceptor Complex.
TLDR
A variety ofAlkenes are compatible in this protocol including aliphatic alkenes, vinyl ethers, enecarbamates, styrenes, and even acrylates, providing diverse β- trifluoromethyl alkynes in good to excellent yields.
An alternative approach of solid-state reaction to prepare nanocrystalline KNbO3
A simple preparation of KNbO3 powders was proposed by an alternative approach of solid-state reaction. Stoichiometric niobium oxalate and potassium acetate were mixed in water and then dried. It was
Thermal Stabilities and the Thermal Degradation Kinetics of Poly(ϵ-Caprolactone)
The thermal degradation behavior of poly(ϵ-caprolactone) (PCL) in nitrogen atmosphere was investigated by thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) techniques and
Prussian blue derived Fe2N for efficiently improving the photocatalytic hydrogen evolution activity of g-C3N4 nanosheets
Prussian blue derived Fe2N nanoparticles to efficiently improve the photocatalytic H2-generation rate over pure g-C3N4 nanosheets.
Copper Nitrate Catalyzed Three-Component One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-Ones
TLDR
An efficient synthesis of 3,4-dihydropyrimidin-2(1H)-ones from aldehydes, 1,3-dicarbonyl compounds, and urea using copper nitrate under refluxing temperature in ethanol proved to be the most efficient.
Synthesis of 6-alkylated phenanthridine derivatives using photoredox neutral somophilic isocyanide insertion.
TLDR
The first example of photoredox neutral, somophilic isocyanide insertions is reported, which provide 6-alkylated phenanthridine derivatives under mild reaction conditions and is considered to be a new synthetic protocol which circumvents the use of stoichiometric oxidants and harsh reaction conditions.
Iminyl-Radicals by Oxidation of α-Imino-oxy Acids: Photoredox-Neutral Alkene Carboimination for the Synthesis of Pyrrolines.
TLDR
This strategy provides a novel catalytic cycle for alkene carboimination through a sequence comprising N-radical generation, iminyl radical cyclization, intermolecular conjugate addition to a Michael acceptor, and single-electron reduction to afford various pyrroline derivatives in an overall redox-neutral process.
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