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The synthesis of new pinene-derived chiral cyclopropylamines and their use in the synthesis of the first asymmetric Alkyl-BIAN ligands (Alkyl-BIAN = bis-(alkylimino)acenaphthenequinone) are reported.
Pyridinoline (Pyr), deoxypyridinoline (D-Pyr), galactosyl-pyridinoline (Gal-Pyr) and glucosyl-galactosyl pyridinoline (GluGal-Pyr) are enzymatic mature pyridinium crosslinks. Generally, only total Pyr and D-Pyr urinary amounts (free+bound forms) are evaluated by HPLC as indices of bone resorption. This report describes the validation of an HPLC-fluorescence… (More)