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Three-component coupling reactions in ionic liquids: One-pot synthesis of isoxazolidines☆
1-Butyl-3-methylimidazolium based ionic liquids are found to accelerate significantly the intermolecular 1,3-dipolar cycloaddition of nitrones derived in situ from aldehydes and phenyl hydroxylamine,… Expand
Lithium Perchlorate Catalyzed Reactions of Indoles: An Expeditious Synthesis of Bis(indolyl)methanes
Lithium perchlorate is found to catalyze efficiently the electrophilic substitution reactions of indoles with aldehydes and ketones in diethyl ether to afford the corresponding bis(indolyl)methanes… Expand
Synthesis of 2-Methoxy 5-nitro9,10-anthraquinone and study of photophysical properties
Literature survey reveal that a good number of Anthracene and substituted Anthracene are potential lasing organic compounds. As per mit suo meada66 9,10-dimethyl and 9,10-diphenyl Anthracenes exhibit… Expand
Synthesis of (+)-lycoricidine by the application of oxidative and regioselective ring-opening of aziridines.
A highly stereoselective total synthesis of (+)-lycoricidine has been described. The salient features of this synthesis are the one-pot elimination followed by allylation reaction, ring-closing… Expand
Montmorillonite clay catalyzed in situ Prins-type cyclisation reaction ☆
Homoallylic alcohols smoothly undergo cross-coupling reactions with aldehydes on the surface of montmorillonite clay to generate 4-hydroxy-2,6-disubstituted tetrahydropyrans in high yields with high… Expand
Scandium Triflate Catalyzed Ferrier Rearrangement: An Efficient Synthesis of 2,3-Unsaturated Glycopyranosides
Scandium(III) trifluoromethanesulfonate is found to catalyze efficiently the O-glycosidation of 3,4,6-tri-O-acetyl-d-glucal with various alcohols and phenols to afford the corresponding… Expand
Lithium Perchlorate Catalyzed Reactions of Indoles: An Expeditious Synthesis of Bis(indolyl)methanes.
Enantioselective Synthesis of ((1R,2R)-Cyclohexane-1,2-diyl)bis(methylene)dimethanesulfonate, a Lurasidone Hydrochloride Intermediate
Abstract A concise, economical, and highly enantioselective synthesis of bismesylate intermediate of lurasidone HCl, an antipsychotic, has been developed. The key steps involved in the synthesis are… Expand
Scandium Triflate Catalyzed Ferrier Rearrangement: An Efficient Synthesis of 2,3-Unsaturated Glycopyranosides.