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Mechanistic aspects of chiral discrimination on modified cellulose.
TLDR
Investigation of chromatographic kinetic parameters reveals that, at low temperature, the second eluted enantiomer undergoes sluggish inclusion interactions, and molecular modeling of (R)- and (S)-diol and the stationary phase suggests that hydrogen bonding is a primary factor in the separation.
Aminosterols from the dogfish shark Squalus acanthias.
TLDR
Seven new aminosterols related to squalamine were isolated from the liver of the dogfish shark Squalus acanthias using spectroscopic methods, including 2D NMR and HRFABMS to determine the structure of the lone spermine conjugate.
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