Alice E. O’Connor

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Two independent mol-ecules of the title solvated complex, [V(C16H14N2O2)O]·CH3OH, also known as [N,N'-bis-(salicyl-idene)ethyl-enedi-amine]-oxidovanadium(IV) or vanadyl salen, crystallize in the asymmetric unit. Each disordered methanol solvent mol-ecule [occupancy ratios 0.678 (4):0.322 (4) and 0.750 (5):0.250 (5)] is linked to a(More)
Recrystallization of [PdCl 2 ([9]aneS 2 O)] ([9]aneS 2 O = 1-oxa-4,7-dithiacyclononane), 1, and [PtCl 2 ([9]aneS 2 O)], 2, by diffusion of Et 2 O vapor into solutions of the complexes in MeNO 2 yielded three phases of 1 and two phases of 2. The known phase of 1, herein designated α-1, was obtained under ambient conditions. A second phase, designated β-1,(More)
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