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Comprehensive study of surface chemistry of MCM-41 using 29Si CP/MAS NMR, FTIR, pyridine-TPD, and TGA
A comprehensive study was conducted on mesoporous MCM-41. Spectroscopic examinations demonstrated that three types of silanol groups, i.e., single, (SiO)3Si-OH, hydrogen-bonded,…
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Rehydration process of milk protein concentrate powder monitored by static light scattering
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Investigation of the microstructure of milk protein concentrate powders during rehydration: alterations during storage.
TLDR
Investigation of the microstructure of rehydrated milk protein concentrate powder particles shows a porous, gel-like structure that restrains the dispersion of individual micelles into the surrounding liquid phase without preventing water penetration and solubilization of nonmicellar components.
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A method for estimating the nature and relative proportions of amorphous, single, and double-helical components in starch granules by (13)C CP/MAS NMR.
TLDR
The method of preparation was found to be more important than the starch botanical origin in determining (13)C NMR spectral features of amorphous samples, and shows that the V-type single-helical component increases with amylose content of starches.
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Rehydration of high-protein-containing dairy powder: Slow- and fast-dissolving components and storage effects
As dissolution of powdered milk proteins is necessary for the expression of their functional properties, it is regarded as a critical property by the dairy industry. However, milk proteins exhibit a…
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Determination of T1rhoH relaxation rates in charred and uncharred wood and consequences for NMR quantitation.
TLDR
A new method for correcting for T1rhoH signal losses in spin counting experiments is developed to deal with the rapidly relaxing component detected in the VSL experiment, which increased the proportion of potential 13C CPMAS NMR signal that can be accounted for by up to 50% for the charred samples.
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Structure and orientation of the pore-forming peptide, melittin, in lipid bilayers.
TLDR
Ten analogues of the 26-residue, bee venom peptide, melittin were synthesized, each with 13C enrichment of a single peptide carbonyl carbon, and it was evident that the peptide was well-aligned in the bilayers and reoriented about the bilayer normal.
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Modelling of post-irradiation events in polymer gel dosimeters.
TLDR
A model of fast exchange of magnetization taking into account ongoing gelation and strengthening of the gelatin matrix as well as the polymerization of the monomers with time is presented and Published data on the changes of T2 in gelatin gels as a function of post-manufacture time are used and fitted closely by the model.
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Analysis of lipoproteins using 2D diffusion-edited NMR spectroscopy and multi-way chemometrics
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Structure of calcium aluminate sulfate Ca4Al6O16S
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