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目的改进2-三氟甲基噻吨-9-酮的合成工艺。方法以邻氨基苯甲酸为原料,经重氮化、还原、偶合和环合四步反应制备2-三氟甲基噻吨-9-酮。结果与结论通过改进合成2-三氟甲基噻吨-9-酮的投料方法和后处理方法,使反应产率由36.8%提高到48%。